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GCMS analysis results for sample AD29667, Jan 2002

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GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036815–000036830

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\29667.D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 21:02 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 24.11 284 562 N.D. 33) Phenanthrene 25.05 178 6463 N.D. 34) Anthracene 25.18 178 1971 N.D. 35) Di-n-butylphthalate 27.04 149 32601 N.D. 36) Fluoranthene 28.76 202 1536 N.D. 39) Pyrene 29.45 202 2682 N.D. 40) Butylbenzylphthalate 31.52 149 1025 N.D. 41) Benzo(a)anthracene 33.02 228 9162 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 10101 N.D. 43) Chrysene 33.10 228 3864 N.D. 45) Di-n-Octylphthalate 35.03 149 1290 N.D. 46) Benzo(b)fluoranthene 36.10 252 1371 N.D. 47) Benzo(k)fluoranthene 36.10 252 2084 N.D. 48) Benzo(a)pyrene 36.96 252 776 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29667.D GCMS1126.M Wed Jan 16 09:08:48 2002 Page 2

NYC-WTC_000036818

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NYC-WTC_000036818Source: NYC Law Department, mirrored locally

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