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GCMS analysis results for sample AD29667, Jan 2002

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GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036815–000036830

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC3101\29667.D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 21:02 2002 Quant Results File: GCMS1126.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Fri Dec 28 15:11:00 2001 Response via Initial Calibration DataAcq Meth GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1308165 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4994839 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.57 164 2444632 20.00 ug/1 0.00 29) Phenanthrene-diO 24.98 188 3622778 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 2180991 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1256702 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 158007 3.97 ug/mL 0.00 Spiked Amount 5.000 Recovery = 79.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.34 74 259 N.D. 3) bis(2-Chloroethyl)ether 11.15 93 567 N.D. 4) 1,3-Dichlorobenzene 11.60 146 299 N.D. 5) 1,4-Dichlorobenzene 11.73 146 573 N.D. 6) 1,2-Dichlorobenzene 12.24 146 124 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.07 117 212 N.D. 11) Nitrobenzene 13.43 77 100 N.D. 12) Isophorone 14.08 82 996 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.19 180 208 N.D. 15) Naphthalene 15.33 128 5112 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.94 162 172 N.D. 20) Dimethylphthalate 20.06 163 965 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.13 152 1541 N.D. 23) Acenaphthene 20.65 153 2046 N.D. 24) 2,4-Dinitrotoluene 21.17 165 241 N.D. 25) Diethylphthalate 22.12 149 4220 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.26 166 1788 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29667.D GCMS1126.M Wed Jan 16 09:08:44 2002 Page 1

NYC-WTC_000036817

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NYC-WTC_000036817Source: NYC Law Department, mirrored locally

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