NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\DEC3101\29667.D Vial: 56
Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 2 21:02 2002 Quant Results File: GCMS1126.RES
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title 209 625/TCLP calibration table
Last Update Fri Dec 28 15:11:00 2001
Response via Initial Calibration
DataAcq Meth GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1308165 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 4994839 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.57 164 2444632 20.00 ug/1 0.00
29) Phenanthrene-diO 24.98 188 3622778 20.00 ug/1 0.00
38) Chrysene-dl2 33.02 240 2180991 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 1256702 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 158007 3.97 ug/mL 0.00
Spiked Amount 5.000 Recovery = 79.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.34 74 259 N.D.
3) bis(2-Chloroethyl)ether 11.15 93 567 N.D.
4) 1,3-Dichlorobenzene 11.60 146 299 N.D.
5) 1,4-Dichlorobenzene 11.73 146 573 N.D.
6) 1,2-Dichlorobenzene 12.24 146 124 N.D.
7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.07 117 212 N.D.
11) Nitrobenzene 13.43 77 100 N.D.
12) Isophorone 14.08 82 996 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 15.19 180 208 N.D.
15) Naphthalene 15.33 128 5112 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.94 162 172 N.D.
20) Dimethylphthalate 20.06 163 965 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 20.13 152 1541 N.D.
23) Acenaphthene 20.65 153 2046 N.D.
24) 2,4-Dinitrotoluene 21.17 165 241 N.D.
25) Diethylphthalate 22.12 149 4220 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 22.26 166 1788 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29667.D GCMS1126.M Wed Jan 16 09:08:44 2002 Page 1
NYC-WTC_000036817
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