Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
NYC-WTC_000036542–000036558Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\JAN0 302\29520.D Vial: 16 Acq On 4 Jan 2002 1:12 am Operator: 209 GALOS Sample gems scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 2:00 2002 Quant Results File: GCMS1126.RES
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Fri Dec 28 15:11:00 2001 Response via Initial Calibration DataAcq Meth GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 1410988 20.00 ug/1 -0.17 10) Naphthalene-d8 15.13 136 5432851 20.00 ug/1 -0.18 17) Acenaphthene-diO 20.40 164 2653891 20.00 ug/1 -0.18 29) Phenanthrene-diO 24.81 188 3977031 20.00 ug/1 -0.18 38) Chrysene-dl2 32.84 240 2350349 20.00 ug/1 -0.19 44) Perylene-dl2 36.91 264 1422203 20.00 ug/1 -0.21
System Monitoring Compounds 37) 2,4-DDD 29.89 235 169303 3.87 ug/mL -0.18 Spiked Amount 5.000 Recovery = 77.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.13 74 212 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 12.82 117 179 N.D. 11) Nitrobenzene 13.15 77 183 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 4604 N.D. ■ 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 19.96 165 185 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.41 153 138 N.D. 24) 2,4-Dinitrotoluene 21.15 165 367 N.D. 25) Diethylphthalate 21.91 149 1220 N.D. 26) 4-Chlorophenyl-phenylether 0.00 2 04 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 29520.D GCMS1126.M Tue Jan 08 10:22:39 2002 Page 1
NYC-WTC_000036544
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NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018123
Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036492
Fragmented page from a DEP environmental sampling record containing partial text and data fields.
Filed in the same folder
NYC-WTC_000036494
Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
Filed in the same folder
NYC-WTC_000036498
Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
Filed in the same folder
NYC-WTC_000036503
Laboratory report documenting GCMS blank analysis for organic compounds conducted on January 4, 2002, showing results below detection limits.
Filed in the same folder