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GCMS analysis results for sample AD29734, Jan 2002

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GCMS analysis report for sample AD29734 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036874–000036887

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN0302\29734.D Vial: 14 Acq On 3 Jan 2002 11:15 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 0:04 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.87 178 779 N.D. 34) Anthracene 24.87 178 779 N.D. 35) Di-n-butylphthalate 26.83 149 36967 N.D. 36) Fluoranthene 28.50 202 408 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.33 149 373 N.D. 41) Benzo(a)anthracene 32.84 228 6340 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 9582 N.D. 43) Chrysene 32.91 228 604 N.D. 45) Di-n-Octylphthalate 34.87 149 1183 N.D. 46) Benzo(b)fluoranthene 35.88 252 1701 N.D. 47) Benzo(k)fluoranthene 35.88 252 3779 N.D. 48) Benzo(a)pyrene 36.74 252 1357 N.D. 49) Indeno(1,2,3-cd)pyrene 40.51 276 281 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.58 276 423 N.D.

(#) = qualifier out of range (m) = manual integration 29734.D GCMS1126.M Tue Jan 15 16:04:39 2002 Page 2

NYC-WTC_000036877

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NYC-WTC_000036877Source: NYC Law Department, mirrored locally

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