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GCMS analysis comments for sample AD29517 re-analysis required, Jan 2002

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.

NYC-WTC_000036656–000036677

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN0302\29517.D Vial: 17 Acq On 4 Jan 2002 2:10 am Operator: 209 GALOS Sample gems scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 10:40 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.87 178 1310 N.D. 34) Anthracene 24.87 178 1310 N.D. 35) Di-n-butylphthalate 26.82 149 14894 N.D. 36) Fluoranthene 28.49 . 202 812 N.D. 39) Pyrene 29.15 202 326 N.D. 40) Butylbenzylphthalate 31.33 149 186 N.D. 41) Benzo(a)anthracene 32.84 228 6233 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 15160 N.D. 43) Chrysene 32.92 228 103 N.D. 45) Di-n-Octylphthalate 34.87 149 421 N.D. 46) Benzo(b)fluoranthene 35.94 252 2347 N.D. 47) Benzo(k)fluoranthene 35.94 252 1486 N.D. 48) Benzo(a)pyrene 36.73 252 772 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 ) Dibenz(a,h)anthracene 0.00 273 0 N.D. 51) Benzo(g,h,i)perylene 41.58 276 215 N.D.

(#) = qualifier out of range (m) = manual integration 29517.D GCMS1126.M Tue Jan 08 10:40:35 2002 Page 2

NYC-WTC_000036659

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NYC-WTC_000036659Source: NYC Law Department, mirrored locally

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