NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\2O9\DATA\DEC13O1\29522.D Vial: 21.
Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS
Sample : gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 10 Permethrin Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
25.12 8.89 ug/1 4401420 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Permethrin/ 390 C21H20C12O3 052645-53-1 64
2 Cyclopropanecarboxylic acid, 3-(2,2 390 C21H20C12O3 051877-74-8 45
3 Hydrazinecarboxamide , 2 - (2,6-dimeth 183 C9H17N3O 057174-11-5 43
4 Benzenemethanol, . alpha .-methyl-. al 198 C14H140 000599-67-7 38
Abundance Scan 2187 (25.119 min): 29522.D (-) m/z 182.95 100.00%
183
5000
165 -----
. 199 221
51 77 . 103121 141. 24.80 25.00 25.20 25.40
------ 11 i~~i 'i 11111111111111111111111111TITTTTTTTTTTTT
0 m/z 198.05 36.45%
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380
Abundance .... ............... #74166: Permethrin “
183
5000
24.80 25.00 25.20 25.40
163 m/z 165.00 21.95%
77
II L
TTTTTTTTpnnT7TTTTp-rrTTTY^^ .II,.
127
l1' " i i" " i" " i
257
TUAODUTTTTTTTTTu
311 354 390
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380
Abundance #53082: Cyclopropanecarboxylic acid. 3-(2,2-dichlorovinyl)-
183
i —
24.80 25.00 25.20 25.40
5000 m/z 184.00 14.68%
163
91 127
| 1109, ......
r '1' i'' ■' i' ‘" i" " r ' " i" '' i'' " i i" " i ‘ " • I ’' "I T’TTIT I‘"‘IOICOUIIITEITTT
m/z—> 4Q 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380
Abundance #18580: Hydrazinecarboxamide, 2-(2,6-dimethylcyclohexyliden J 1.
183 24.80 25.00 25.20 25.40
m/z 77.05 11.06%
126
61
5000
108
m/z—>
TTpT-rrp-rrrprr TT ।।
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380
।111 11 i i । । । TTTTT’TT 111 111 j 11111 1
—24.80 25.00 25.20 25.40
29522.D GCMS1126.M Tue Jan 08 10:54:33 2002 Page 10
NYC-WTC_000036743
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