Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 14, 2001.
NYC-WTC_000036729–000036751Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU-1\2O9\DATA\DEC13O1\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Phenol, 3,5-bis(1,1-dimethylet Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
24.36 2.41 ug/1 1191750 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenol, 3,5-bis(1,1-dimethylethyl)- 206 C14H22O 001138-52-9 38 2 Benzene, methoxybis (1 -methylpropyl) 220 C15H240 054852-59-4 37 3 Methyl 4 -tert-butylbenzoate 192 C12H1602 026537-19-9 30 4 Amiphenazole 191 C9H9N3S 000490-55-1 30 'Abundance Scan 2104 (24.357 min): 29522.0 (-) m/z 177.05 100.00% 117 191
5000- 41 55 233 163 206 69 91 262 150 TTum—umT ■ ■ | < 1 -r | ■ . I 105 121 219 137 24.00 24.20 24.40 24.60 1 , 247 -r —LllAA— — 4l411al,4all, l , + 11‘ TTT -------- m/ z 191.00 94.47% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #24419: Phenol, 3,5-bis(1,1-dimethylethyl)- 191
57 _ _____ — 5000 . । 1 3 i ( j f i .
24.00 24.20 24.40 24.60 206 m/ z 41.05 34.45% 73 197 121 135 147 163 176 1 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #27727: Benzene. methoxybis(1-methylpropyl)- 177 —_ U 191 TT Ir t 24.00 24.20 24.40 24.60 5000 m/z 163.00 33.42%
107 121 135147 163 205 2^0
m/z-> Abundance 40 60 80 100 120 140 160 180 200 #20770: Methyl 4-tert-butylbenzoate 177 220 240 260 A' I ' ' ■ ' i ' ' ' • i ' ' 24.00 24.20 24.40 24.60 J
m/z 206.10 32.25% 5000- 149 59 91 105 117 161 192 I J III. ■ ■ i ' . II T > . . I » , I ■ ' ■ ' i ' ' 1 1 । 1 1 ' i ' ' ' ' i ' ' ' ' i ' m/z-> 4C 60 80 100 120 140 160 180 200 220 240 260 24.00 24.20 24.40 24.60
29522.D GCMS1126.M Tue Jan 08 10:54:28 2002 Page 9
NYC-WTC_000036742
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NYC-WTC_000036752
Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder