Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 14, 2001.
NYC-WTC_000036729–000036751Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC1301\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************** * * * * * * ** * * * * * * * * ** ** * * * * * Peak Number 6 IH-Pyrazole, 4,5-dihydro-3, 5,5 Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
22.93 2.26 ug/1 1120690 Phenanthrene-diO 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1H-Pyrazole, 4,5-dihydro-3,5,5-trim 112 C6H12N2 003975-85-7 32 2 Fenproporex 188 C12H16N2 015686-61-0 23 3 2 -Oxazolidinethione , 4,4-dimethyl - 131 C5H9NOS 054013-55-7 22 4 4-Metljyltetrahydro-1,3-oxazine-2-th 131 C5H9NOS 014760-60-2 12 ‘Abundance Scan 1949 (22.934 min): 29522.D (-) m/ z 97.05 100.00% 97 131 5000 41 56
72 J TEE’" I TIT ' 1 1 i ! 88 113 22.60 22.80 23.00 23.20 - +— „ 153 164 177186 207 i TTTI—ET"nuup TTTTTT m/z 131.00 64.21% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #2543: 1H-Pyrazole, 4,5-dihydro-3,5,5-trimethyl- 97
5000 56 22.60 22.80 23.00 23.20 112 m/ z 56.00 45.38% 27 42 I . ‘ 11 •' ’ I 70 83 | I I . ! | I ! ( , | ll . > | I . .. | ( | | 14| | | . TT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #19928: Fenproporex 97 U TI0n/n/mTu.m TTTui 22.60 22.80 23.00 23.20 56 5000- m/z 41.05 43.88%
42 68 115 132 U6 173 Tri TT I" " I" " I" " I i1111111" i'111 r1111 i"' 11"' 11 “11"111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #5592: 2-Oxazolidinethione, 4,4-dimethyl- i ‘ ■ i 131 22.60 22.80 23.00’ 23.20 m/z 54.00 26.57% 56 5000- 42 100 116 TTTTTTTTT mmmmmm 30 । 72 "'I'“'I•*''11 '••| | " I HIt| !IIIrII.IUII|IIII |III m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 22.60 22.80 23.00 23.20
29522.D GCMS1126.M Tue Jan 08 10:54:12 2002 Page 6
NYC-WTC_000036739
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NYC-WTC_000036752
Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder