Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 14, 2001.
NYC-WTC_000036729–000036751Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU-1\209\DATA\DEC1301\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT:P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzene, methoxybis(1-methylpr Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
21.65 2.11 ug/1 1081830 Acenaphthene-dl0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzene, methoxybis (1-methylpropyl) 220 C15H240 054852-59-4 25 2 Umbellif erone + BSTFA 234 C12H1403Si 000000-00-0 22 3 Diethylphosphinothioic azide 163 C4H10N3PS 058347-14-1 14 4 Ethyl 4 -aetetylbenzoate 192 C11H1203 038430-55-6 14 Abundance Scan 1809 (21.649 min): 29522.D (-) m/z 163.05 100.00% I। 163 177 i 41 219 234 191 5000- 135 149 55 67 91 77 107 121 207 —Pt . ' 4 jln 4 il 4ll l . hi 1 Jl MU —... 21.40 21.60 21.80 22.00
m/z-> I......... I 20 40 — 60 —l 80 100 120140 160 180 200 220 T 240 m/z 177.05 98.13% Abundance #27727: Benzene, methoxybis(l-methylpropyl)- 177 191
5000 ■ ■ i ■ ■ ■ ■ i ■ 1 21.40 21.60 21.80 22.00 m/z 41.05 70.47% 107 ' . 121 135 I I tI 147 I. 163 I | II 205 22 ... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #30681; Umbelliferone + BSTFA 219 163 234 21.40 21.60 21.80 22.00 5000 m/z 219.05 66.87% 73
I 45 89 19% 191 | i 151 I 175 206 i ■ ■ ■ ■ i ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #13085: Diethylphosphinothioic azide ....... A ' ' I ' ’ ■ ' I ' ' * ' I ’ ■ ' • I ' • 163 21.40 21.60 21.80 22.00 121 m/z 234.15 61.25% 5000- 135 46 93 27 65 79
i ■ ■ ' ■ i III I 107 ■ ' i ' ' ' ' i ' ' ' ■ i ' ' ' ' i ' ■ ' ' i ' ' m/z~> 20 40 60 80 100 120 140 160 180 200 22( 240 21.40 21.60 21.80 22.00
29522.D GCMS1126.M Tue Jan 08 10:54:07 2002 Page 5
NYC-WTC_000036738
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NYC-WTC_000036752
Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder