GCMS calibration table for TCLP method, Dec 2001

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Library Search Compound Report

Data File : M:\INSTRU~1\2O9\DATA\DEC13O1\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Propanenitrile, 3,3‘-iminobis- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

18.19 1.05 ug/1 539198 Acenaphthene -dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanenitrile; 3,3'-iminobis- 123 C6H9N3 000111-94-4 52 2 1-Methyl-IH-V; 2,4-triazole 83 C3H5N3 006086-21-1 27 3 4H-1,2,4-Triazole, 4-methyl- 83 C3H5N3 010570-40-8 25 4 2 -Aminoimidazole 83 C3H5N3 _______ 000000-00-0 12 •Abundance Scan 1432 (18.188 min): 29522.D (-) m/z 83.05 100.00% i 42 $ l 54 5000 / Q * 1 1 'I ‘ 1.T I 17.80 18.00 18.20 18.40 18.60

m/z-> 10 20 30 +1 1 40 50 60 70 69 75 | 1 ’’i ■ ■ ' ■ I ' 80 90 100 -9 110 120123 130 m/z 42.05 90.40% Abundance #4016: Propanenitrile, 3,3'-iminobis- 42

5000 54 - 17.80 18.00 18.20 18.40 18.60 30 m/z 54.00 54.10% 83

mz-> 4 10 20 30 ‘It "tIl 40 50 60 70 80 66........ , I, 90 ............... 123 100 110 120 130 Abundance #62695: 1 -Methyl-1H-1.2.4-triazole 83 i

17.80 18.00 18.20 18.40 18.60 56

0 5000 I

27 40 ' 1 i ■ • • ' i ’ ' ■ ' I ' ■ 1 ' i 1 ' ' ' t ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #509: 4H-1,2,4-Triazole, 4-methyl- 83 17.80 18.00 18.20 18.40 18.60 27 m/ z 41. • 5000 42 55 I

m/z-> 10 20 30 40 —4 50 60 • i ■ ■ • > । > l ■ • i > ■ • • i ■ • • • i • ■ ■ ■ i ■ • ■ > i ■ 70 80 90 100 110 120 130 17.80 18.00 18.20 18.40 18.60

29522.D GCMS1126.M Tue Jan 08 10:54:02 2002 Page 4

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