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GCMS analysis data for sample AD29466, Jan 2002

Machine-extracted title · confidence 95%

Raw GCMS analysis data and chromatogram details for sample AD29466 including surrogate recovery results.

NYC-WTC_000036603–000036613

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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Scanned page image, NYC-WTC_000036608
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC1301\29464.D Vial: 14 Acq On 13 Dec 2001 10:34 pm Operator: 209 GALOS Sample gems scan 12/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak . peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 312 rVB 453101 1198414 13.61% 2.473% 2 11.330 681 685 690 rBV 275912 554616 6.30% 1.145% 3 11.413 690 694 714 rVB 274591 703995 7.99% 1.453% 4 11.670 714 722 739 rBV2 2791411 7295779 82.84% 15.056% 5 15.278 1109 1115 1134 rBV 3756289 8267894 93.88% 17.063%

6 20.556 1683 1690 1714 rBV 3818459 8806713 100.00% 18.174% 7 24.972 2164 2171 2183 rBV2 3673770 8343539 94.74% 17.219% 8 25.119 2183 2187 2200 rVB 35563 122827 1.39% 0.253% 9 30.049 2718 2724 2735 rBV 470305 947400 10.76% 1.955% 10 33.014 3038 3047 3070 rBV2 2731117 6646624 75.47% 13.717%

11 33.290 3072 3077 3092 rVB 78454 227155 2.58% 0.469% 12 37.099 3484 3492 3518 rBV2 1882580 5341532 60.65% 11.023%

Sum of corrected areas: 48456488

29464.D GCMS1126.M Fri Dec 21 13:09:20 2001

NYC-WTC_000036608

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NYC-WTC_000036608Source: NYC Law Department, mirrored locally

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