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GCMS analysis results for sample AD29787, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29787 conducted on January 7, 2002.

NYC-WTC_000036995–000037006

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29787.D Vial: 12 Acq On 15 Dec 2001 1:16 pm Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 291 rBV 337926 892446 14.34% 2.760% 2 • 7.741 291 294 311 rVB 35516 144205 2.32% 0.446% 3 11.340 682 686 691 rBV 99715 225358 3.62% 0.697% 4 11.422 691 695 711 rVB 108223 323641 5.20% 1.001% 5 11.670 715 722 740 rBV 1807296 4790141 76.94% 14.813%

6 15.278 1109 1115 1133 rBV 2570601 5746898 92.31% 17.772% 7 20.547 1683 1689 1709 rBV 2738931 6225543 100.00% 19.252% 8 24.972 2165 2171 2185 rBV2 2528258 5730076 92.04% 17.720% 9 25.119 2185 2187 2200 rVB2 23509 78666 1.26% 0.243% 10 30.049 2719 2724 2733 rBV 378352 785973 12.62% 2.431%

11 33.005 3040 3046 3066 rBV2 1706102 4225130 67.87% 13.066% 12 33.290 3072 3077 3086 rVB2 25302 62708 1.01% 0.194% 13 37.100 3485 3492 3516 rBV2 107005C 3106195 49.89% 9.606%

Sum of corrected areas: 32336980

29787.D GCMS1126.M Fri Dec 28 13:22:26 2001

NYC-WTC_000037000

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NYC-WTC_000037000Source: NYC Law Department, mirrored locally

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