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GCMS analysis results for sample AD29925, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AD29925 conducted on January 7, 2002.

NYC-WTC_000036972–000036982

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File : C:\HPCHEM\1\DATA\DEC1401\29925.D Vial: 13 Acq On 15 Dec 2001 2:15 pm Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.600 273 278 291 rBV 369004 1045433 16.31% 3.089% 2 7.738 291 293 301 rVB 28152 76430 1.19% 0.226% 3 11.346 682 686 691 rBV 101491 227762 3.55% 0.673% 4 11.428 691 695 714 rVB 109868 341914 5.33% 1.010% 5 11.676 714 722 740 rBV2 1738967 4936655 77.00% 14.586%

6 15.275 1109 1114 1133 rBV 2657101 5917046 92.30% 17.483% 7 20.554 1683 1689 1712 rBV 3053386 6410948 100.00% 18.942% 8 24.978 2164 2171 2183 rBV2 2570639 6033547 94.11% 17.827% 9 25.125 2184 2187 2202 rVB3 26601 97396 1.52% 0.288% 10 26.989 2385 2390 2400 rBV 29534 70543 1.10% 0.208%

11 30.055 2719 2724 2733 rBV 412041 840820 13.12% 2.484% 12 33.011 3039 3046 3069 rBV2 1828207 4479502 69.87% 13.235% 13 37.106 3484 3492 3516 rBV2 1119750 3366773 52.52% 9.948%

Sum of corrected areas: 33844769

29925.D GCMS1126.M Fri Dec 28 13:27:48 2001

NYC-WTC_000036977

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NYC-WTC_000036977Source: NYC Law Department, mirrored locally

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