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GCMS analysis data for sample AD29517, Jan 2002

Machine-extracted title · confidence 95%

Raw GCMS analysis data and chromatogram details for sample AD29517 including surrogate recovery results.

NYC-WTC_000036645–000036655

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\l\DATA\DEC1301\29466.D Vial: 12 Acq On : 13 Dec 2001 8:37 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 299 rBV 297912 763369 8.19% 1.568% 2 11.331 681 685 690 rBV 224099 448672 4.82% 0.922% 3 11.413 690 694 714 rVB 212778 565046 6.07% 1.161% 4 11.670 714 722 739 rBV2 2989400 7448644 79.96% 15.299% 5 15.278 1108 1115 1133 rBV 3905756 8752480 93.95% 17.977%

6 20.557 1682 1690 1715 rBV 4109566 9315768 100.00% 19.134% 7 24.973 2164 2171 2184 rBV2 3929325 8722311 93.63% 17.915% 8 25.119 2184 2187 2196 rVB 32315 94600 1.02% 0.194% 9 30.049 2718 2724 2732 rBV 326363 668544 7.18% 1.373% 10 33.015 3039 3047 3071 rBV2 2652029 6575860 70.59% 13.506%

11 33.290 3072 3077 3085 rW 40451 104234 1.12% 0.214% 12 37.100 3484 3492 3517 rBV2 1775329 5227683 56.12% 10.737%

Sum of corrected areas: 48687211

29466.D GCMS1126.M Fri Dec 21 13:10:28 2001

NYC-WTC_000036650

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NYC-WTC_000036650Source: NYC Law Department, mirrored locally

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