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GCMS analysis comments for sample AD29524, Jan 2002

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29524 indicating no unusual compounds detected.

NYC-WTC_000036570–000036580

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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Scanned page image, NYC-WTC_000036575
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NYC 9/11 Public Portal Document

LSC Area Percent Report

-Data File : C:\HPCHEM\l\DATA\DEC1301\29524.D Vial: 13 Acq On : 13 Dec 2001 9:35 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : ’ Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.589 273 277 311 rBV 535506 1408564 15.15% 2.743% 2 11.326 680 684 690 rBV 399640 822664 8.85% 1.602% 3 11.408 690 693 713 rVB 405980 1005325 10.82% 1.958% 4 11.675 713 722 739 rBV2 2822329 8050740 86.61% 15.676% 5 15.273 1108 1114 1133 rBV 4131302 8813014 94.81% 17.160%

6 20.552 1682 1689 1707 rBV 4262125 9295408. 100.00% 18.100% 7 24.977 2164 2171 2183 rBV2 3976958 8848807 95.20% 17.230% 8 25.115 2183 2186 2198 rVB2 35101 123440 1.33% 0.240% 9 30.044 2718 2723 2735 rBV 452816 958802 10.31% 1.867% 10 33.010 3037 3046 3070 rBV2 2791214 6596391 70.96% 12.844%

11 33.294 3071 3077 3086 rW 53639 154152 1.66% 0.300% 12 . 35.562 3317 3324 3332 rBV2 30398 101965 1.10% 0.199% 13 37.104 3483 3492 3513 rBV2 1785278 5177341 55.70% 10.081%

Sum of corrected areas: 51356613

29524.D GCMS1126.M Fri Dec 21 13:16:20 2001

NYC-WTC_000036575

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NYC-WTC_000036575Source: NYC Law Department, mirrored locally

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