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GCMS analysis comments for sample AD29464 with phthalate detection, Jan

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29464 noting bis(2-Ethylhexyl)phthalate at 0.48 ug/L.

NYC-WTC_000036592–000036602

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC1301\29518.D Vial: 10 Acq On : 13 Dec 2001 6:40 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.595 274 278 291 rBV 368050 1000799 11.54% 2.119% 2 7.742 292 294 313 rVB 37797 139444 1.61% 0.295% 3 11.331 681 685 690 rBV 546785 1107072 12.77% 2.344% 4 11.414 690 694 713 rVB 527451 1331821 15.36% 2.819% 5 11.671 713 722 740 rBV2 2657010 7699753 88.80% 16.300%

6 15.279 1109 1115 1133 rBV 3703002 8003089 92.29% 16.942% 7 20.557 1683 1690 1706 rBV 3890170 8671337 100.00% 18.356% 8 24.973 2164 2171 2183 rBV2 3560556 7905931 91.17% 16.736% 9 25.120 2183 2187 2197 rVB2 31695 107353 1.24% 0.227% 10 30.050 2716 2724 2733 rBV 416010 845486 9.75% 1.790%

11 33.006 3037 3046 3062 rBV2 2409082 5738955 66.18% 12.149% 12 33.290 3071 3077 3084 rBV 64411 153863 1.77% 0.326% 13 37.100 3484 3492 3517 rBV2 1583539 4534122 52.29% 9.598%

Sum of corrected areas: 47239025

29518.D GCMS1126.M Fri Dec 21 13:12:42 2001

NYC-WTC_000036597

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NYC-WTC_000036597Source: NYC Law Department, mirrored locally

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