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GCMS comments for sample AD29521, Jan 2002

Machine-extracted title · confidence 95%

Laboratory commentary confirming no unusual compounds detected in sample AD29521 during GCMS scan on January 4, 2002.

NYC-WTC_000036530–000036541

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘•Data File : C:\HPCHEM\1\DATA\DEC1301\29521.D Vial: 8 Acq On : 13 Dec 2001 4:42 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 273 278 291 rBV 467945 1204405 13.55% 2.457% 2 7.736 291 293 310 rVB 38968 151644 1.71% 0.309% 3 9.224 452 455 473 rBV 32881 146270 1.65% 0.298% 4 11.326 680 684 690 rBV 445445 927959 10.44% 1.893% 5 11.409 690 693 713 rVB 460493 1130127 12.71% 2.305%

6 11.675 713 722 739 rBV2 2710236 7810789 87.85% 15.934% 7 15.273 1108 1114 1133 rBV 3898789 8353163 93.95% 17.041% 8 20.552 1682 1689 1708 rBV 4106239 8890969 100.00% 18.138% 9 24.977 2164 2171 2183 rBV2 3644601 8325006 93.63% 16.983% 10 25.124 2183 2187 2196 rVB 32261 102019 1.15% 0.208%

11 30.054 2718 2724 2731 rBV 425813 908779 10.22% 1.854% 12 33.010 3037 3046 3068 rBV2 2584343 6176550 69.47% 12.600% 13 35.562 3319 3324 3335 rBV2 46302 154754 1.74% 0.316% 14 37.104 3484 3492 3513 rBV2 1653622 4736988 53.28% 9.663%

Sum of corrected areas: 49019422

29521 .D GCMS1126.M Fri Dec 21 13:15:06 2001

NYC-WTC_000036535

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NYC-WTC_000036535Source: NYC Law Department, mirrored locally

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