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GCMS analysis comments for sample AD29518 with phthalate detection, Jan

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29518 noting bis(2-Ethylhexyl)phthalate at 0.44 ug/L.

NYC-WTC_000036581–000036591

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\l\DATA\DEC1301\29463.D Vial: 11 Acq On : 13 Dec 2001 7:38 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 278 311 rVB 430768 1137235 12.60% 2.371% 2 11.331 681 685 690 rBV 339735 682642 7.56% 1.423% 3 11.413 690 694 714 rVB 324079 831374 9.21% 1.733% 4 11.670 714 722 740 rBV2 2860492 7465782 82.72% 15.567% 5 15.278 1109 1115 1133 rBV 3863452 8435027 93.46% 17.588%

6 20.557 1683 1690 1721 rBV 4043007 9024915 100.00% 18.818% 7 24.973 2165 2171 2183 rBV2 3782757 8420591 93.30% 17.558% 8 25.120 2183 2187 2195 rVB2 32549 102818 1.14% 0.214% 9 30.049 2719 2724 2734 rBV 444001 905655 10.04% 1.888% 10 33.005 3037 3046 3070 rBV2 2458859 6214885 68.86% 12.959%

11 37.100 3484 3492 3518 rBV2 1623146 4738535 52.51% 9.880%

Sum of corrected areas: 47959459

29463.D GCMS1126.M Fri Dec 21 13:07:49 2001.

NYC-WTC_000036586

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NYC-WTC_000036586Source: NYC Law Department, mirrored locally

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