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GCMS analysis results for sample AD29664, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of sample AD29664 conducted January 9, 2002, reporting unknown compounds and surrogate recovery at 78%.

NYC-WTC_000037188–000037196

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\1\DATA\DEC1401\29664.D Vial: 16 Acq On 15 Dec 2001 5:10 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 291 rBV 296171 795888 12.61% 2.487% 2 11.363 684 688 693 rBV 26323 72642 1.15% 0.227% 3 11.446 693 697 7 05 rW 25300 76750 1.22% 0.240% 4 11.675 716 722 746 rBV 1697148 4638244 73.51% 14.491% 5 15.274 1109 1114 1134 rBV 2601884 5790328 91.77% 18.091%

6 20.552 1683 1689 1711 rBV 2910157 6309295 100.00% 19.712% 7 24.977 2164 2171 2184 rBV2 2449106 5820531 92.25% 18.185% 8 25.124 2184 2187 2200 rVB3 24295 85086 1.35% 0.266% 9 30.054 2719 2724 2734 rVB 329548 701562 11.12% 2.192% 10 33.010 3039 3046 3060 rBV 1811177 4325843 68.56% 13.515%

11 33.295 3072 3077 3087 rVB2 37436 118420 1.88% 0.370% 12 37.095 3484 3491 3514 rBV2 1077438 3272727 51.87% 10.225%

Sum of corrected areas: 32007316

29664.D GCMS1126.M Fri Dec 28 13:07:58 2001

NYC-WTC_000037193

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NYC-WTC_000037193Source: NYC Law Department, mirrored locally

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