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GCMS analysis results for sample AD29733, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29733 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037177–000037187

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29733.D Vial: 20 Acq On 15 Dec 2001 9:03 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.594 274 2 78 300 rBV 370510 989595 13.36% 2.631% 2 11.349 683 687 692 rBV 48184 116031 1.57% 0.308% 3 11.431 692 696 704 rVB 49715 127917 1.73% 0.340% 4 11.670 716 722 742 rBV 2170652 5357825 72.35% 14.242% 5 15.278 1109 1115 1134 rBV 2967518 6738969 91.00% 17.913%

6 20.556 1683 1690 1707 rBV 3235676 7405760 100.00% 19.686% 7 22.071 1848 1855 1863 rBV 34520 100218 1.35% 0.266% 8 24.972 2165 2171 2184 rBV2 3028482 6980341 94.26% 18. 555% 9 26.992 2384 2391 2400 rBV 33449 82500 1.11% 0.219% 10 30.049 2719 2724 2733 rBV 417276 837908 11.31% 2.227%

11 33.005 3040 3046 3070 rBV2 2043602 5189108 70.07% 13.794% 12 37.099 3485 3492 3512 rBV 1253703 3693697 49.88% 9.818%

Sum of corrected areas: 37619869

29733.D GCMS1126.M Fri Dec 28 13:11:05 2001

NYC-WTC_000037182

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NYC-WTC_000037182Source: NYC Law Department, mirrored locally

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