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GCMS analysis comments for sample AD29087, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29087 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.

NYC-WTC_000035876–000035887

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1301\29087.D Vial: 15 Acq On : 13 Dec 2001 10:48 am Operator: 209 GALOS Sample : gems scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.598 274 278 300 rBV 370834 1028155 12.83% 2.532% 2 11.344 682 686 692 rBV 51481 127234 1.59% 0.313% 3 11.426 692 695 710 rVB 58649 177149 2.21% 0.436% 4 11.674 716 722 745 rBV 2224679 5689682 71.01% 14.013% 5 15.273 1109 1114 1133 rBV 3310100 7262027 90.63% 17.886%

6 20.552 1683 1689 1717 rBV 3742244 8012741 100.00% 19.735% 7 24.977 2164 2171 2183 rBV2 3349750 7445192 92.92% 18.337% 8 30.053 2718 2724 2731 rBV 479332 1026194 12.81% 2.527% 9 32.762 3009 3019 3032 rBV 44899 160486 2.00% 0.395% 10 33.009 3038 3046 3062 rBV2 2271027 5358095 66.87% 13.196%

11 33.285 3071 3076 3087 rVB 51142 130425 1.63% 0.321% 12 37.095 3483 3491 3507 rBV2 1441612 4185252 52.23% 10.308%

Sum of corrected areas: 40602632

29087.D GCMS1126.M Thu Dec 13 14:44:48 2001

NYC-WTC_000035881

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NYC-WTC_000035881Source: NYC Law Department, mirrored locally

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