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GCMS analysis results for sample AD29782, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29782 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037166–000037176

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC1401\29782.D Vial: 22 Acq On 15 Dec 2001 11:00 pm Operator: 209 GALOS Sample gems scan 12/10 a Inst : GC/MS 209 Mise . Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 308 rBV 241564 812095 14.48% 2.896% 2 11.345 682 686 691 rBV 93186 215405 3.84% 0.768% 3 11.427 691 695 715 rVB 105594 348424 6.21% 1.242% 4 11.666 715 721 747 rBV 1420609 4253828 75.87% 15.169% 5 15.274 1109 1114 1133 rBV 2214546 5060727 90.26% 18.046%

6 20.553 1683 1689 1712 rBV 2515110 5606981 100.00% 19.994% 7 24.968 2164 2170 2183 rBV2 2077074 4938254 88.07% 17.610% 8 30.054 2718 2724 2733 rBV 323078 690533 12.32% 2.462% 9 33.010 3039 3046 3066 rBV2 1418662 3551073 63.33% 12.663% 10 37.096 3483 3491 3514 rBV2 863048 2565781 45.76% 9.149%

Sum of corrected areas: 28043101

29782.D GCMS1126.M Fri Dec 28 13:12:11 2001

NYC-WTC_000037171

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NYC-WTC_000037171Source: NYC Law Department, mirrored locally

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