GCMS analytical comments identifying dimethylbenzenesulfonamide, Jan 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC1401\26473.D Vial: 44 Acq On 16 Dec 2001 8:42 am Operator: 209 GALOS Sample gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.600 274 278 299 rBV 212194 703598 13.01% 2.596% 2 11.666 716 721 753 rBV 1356307 3981412 73.62% 14.688% 3 15.274 1109 1114 1135 rBV 2157927 5056517 93.50% 18.654% 4 20.553 1682 1689 1711 rBV 2388074 5407980 100.00% 19.951% 5 24.969 2164 2170 2185 rBV2 2128946 5003377 92.52% 18.458%

6 30.055 2718 2724 2735 rBV 267351 563146 10.41% 2.078% 7 33.002 3039 3045 3071 rBV2 1429265 3691937 68.27% 13.620% 8 33.286 3071 3076 3085 rW 42772 117436 2.17% 0.433% 9 37.096 3484 3491 3513 rBV2 854787 2581056 47.73% 9.522%

Sum of corrected areas: 27106459

26473.D GCMS1126.M Wed Jan 30 11:46:03 2002

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