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GCMS analysis results, sample AD29666, January 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.

NYC-WTC_000036831–000036841

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File C:\HPCHEM\l\DATA\DEC3101\29666.D Vial: 64 Acq On 3 Jan 2002 3:59 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 275 279 292 rBV 254452 910632 10.19% 2.027% 2 11.124 658 662 673 rBV 80095 228027 2.55% 0.508% 3 11.675 717 722 759 rBV 2069028 6933952 77.56% 15.434% 4 14.310 1004 1009 1020 rVB2 63307 166690 1.86% 0.371% 5 15.283 1109 1115 1136 rBV 2949604 8423756 94.22% 18.750%

6 20.562 1683 1690 1714 rBV 3493231 8940567 100.00% 19.901% 7 24.987 2165 2172 2204 rBV2 2674743 8335053 93.23% 18.553% 8 30.063 2718 2725 2735 rBV 312065 729553 8.16% 1.624% 9 33.019 3038 3047 3073 rBV2 2078301 6112944 68.37% 13.607% 10 37.114 3486 3493 3513 rBV2 1139274 4144334 46.35% 9.225%

Sum of corrected areas: 44925508

29666.D GCMS1126.M Wed Jan 16 14:45:24 2002

NYC-WTC_000036836

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NYC-WTC_000036836Source: NYC Law Department, mirrored locally

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