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GCMS analysis results for sample AD30486, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AD30486 including DDD surrogates on January 18, 2002.

NYC-WTC_000017097–000017107

Folder label: “GCMS X 12/14/01 A 1/1/02

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Scanned page image, NYC-WTC_000017102
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\ 1\DATA\DEC3101\30486.D Vial: 21 Acq Oh 1 Jan 2002 6:23 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.611 276 280 293 rBV 376320 1017282 14.12% 2.886% 2 7.749 293 295 313 rVB2 38921 153738 2.13% 0.436% 3 11.678 718 723 740 rBV 1953548 5305669 73.67% 15.053% 4 15.277 1110 1115 1138 rBV 2534341 6718047 93.28% 19.060% 5 20.564 1684 1691 1716 rBV 2703713 7202309 100.00% 20.434%

6 24.989 2166 2173 2217 rBV2 2032825 6785747 94.22% 19.252% 7 30.066 2720 2726 2735 rBV 310423 721439 10.02% 2.047% 8 32.738 3011 3017 3028 rBV2 24298 76664 1.06% 0.218% 9 33.022 3042 3048 3069 rBV2 1475767 4423161 61.41% 12.549% 10 37.117 3487 3494 3516 rBV 731870 2842643 39.47% 8.065%

Sum of corrected areas: 35246699

30486.D GCMS1126.M Tue Jan 15 14:50:58 2002

NYC-WTC_000017102

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NYC-WTC_000017102Source: NYC Law Department, mirrored locally

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