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GCMS analysis results for sample AD30350, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AD30350 including DDD surrogates on January 18, 2002.

NYC-WTC_000017069–000017078

Folder label: “GCMS X 12/14/01 A 1/1/02

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Scanned page image, NYC-WTC_000017074
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC3101\30350.D Vial: 18 Acq On 1 Jan 2002 3:29 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.611 276 280 290 rBV 375064 977546 14.39% 2.865% 2 7.730 290 293 315 rVB 99841 399208 5.88% 1.170% 3 11.678 718 723 759 rBV 1867472 5121408 75.38% 15.011% 4 15.277 1110 1115 1135 rBV 2440781 6314520 92.95% 18.508% 5 20.564 1684 1691 1715 rBV 2512014 6793771 100.00% 19.912%

6 24.989 2166 2173 2212 rBV2 1901132 6457539 95.05% 18.927% 7 30.066 2720 2726 2740 rBV 360295 851611 12.54% 2.496% 8 33.022 3042 3048 3074 rBV2 1420424 4391300 64.64% 12.871% 9 37.116 3487 3494 3515 rBV2 718385 2811493 41.38% 8.240%

Sum of corrected areas: 34118396

30350.D GCMS1126.M Tue Jan 15 14:48:38 2002

NYC-WTC_000017074

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NYC-WTC_000017074Source: NYC Law Department, mirrored locally

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