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GCMS analysis log for sample AD30711, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.

NYC-WTC_000018142–000018154

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018147
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\DEC3 10130711.D Vial: 34 Acq On 1 Jan 2002 8:55 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.622 276 281 295 rBV 221036 736841 10.70% 2.222% 2 11.129 658 663 676 rBV 50021 137739 2.00% 0.415% 3 11.670 718 722 742 rBV 1691154 4847698 70.41% 14.621% 4 14.305 1004 1009 1020 rVB 54072 143495 2.08% 0.433% 5 15.278 1110 1115 1152 rBV 2203568 6232523 90.53% 18.798%

6 17.454 1346 1352 1363 rBV 58504 148451 2.16% 0.448% 7 20.281 1654 1660 1667 rVB2 44995 89823 1.30% 0.271% 8 20.557 1684 1690 1722 rBV 2424631 6884752 100.00% 20.765% 9 24.991 2166 2173 2211 rBV2 1821192 6349865 92.23% 19.152%. 10 30.068 2720 2726 2740 rBV 293550 685951 9.96% 2.069%

11 33.024 3042 3048 3073 rBV2 1339851 4220676 61.30% 12.730% 12 37.118 3487 3494 3531 rBV2 644319 2678021 38.90% 8.077%

Sum of corrected areas: 33155835

30711.D GCMS1126.M Wed Jan 23 08:38:37 2002

NYC-WTC_000018147

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NYC-WTC_000018147Source: NYC Law Department, mirrored locally

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