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GCMS analysis results for sample AD31640, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31640 conducted on February 11, 2002.

NYC-WTC_000049762–000049773

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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Scanned page image, NYC-WTC_000049767
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\JAN0 302\31640.D Vial: 36 Acq On 4 Jan 2002 8:38 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.749 73 77 84 rBV 35707 70746 1.45% 0.296% 2 7.466 260 264 275 rBV 350566 885153 18.20% 3.707% 3 7.604 275 279 296 rVB 60073 246548 5.07% 1.033% 4 11.524 701 706 725 rBV 1501614 3731485 76.72% 15.628% 5 14.168 989 994 999 rBV 120271 221901 4.56% 0.929%

6 15.122 1092 1098 1115 rBV 2265055 4727397 97.19% 19.798% 7 20.383 1665 1671 1685 rBV 2255187 4863975 100.00% 20.370% 8 24.798 2146 2152 2165 rBV2 1973742 4321303 88.84% 18.098% 9 26.827 2368 2373 2383 rVB 29869 58454 1.20% 0.245% 10 29.884 2700 2706 2712 rBV 299447 588240 12.09% 2.464%

11 32.831 3021 3027 3041 rBV2 1085394 2480830 51.00% 10.390% 12 36.898 3463 3470 3491 rBV 621630 1681549 34.57% 7.042%

Sum of corrected areas: 23877581

31640.D GCMS1126.M Fri Feb 01 11:14:06 2002

NYC-WTC_000049767

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NYC-WTC_000049767Source: NYC Law Department, mirrored locally

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