GCMS analysis comments for sample AD29464 with phthalate detection, Jan

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\29518.D Vial 10 Acq On : 13 Dec 2001 6:40 pm Operator 209 GALOS Sample : gems scan 12/6 Inst GC/MS 209 Mise : Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.33 2.88 ug/1 1107070 1,4-Dichlorobenzene-d4 11.67

Hit# of .5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2/methoxy-l-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1/- oxybis- 134 C6H14O3 000110-98-5 56 3 2-Butanol, 3,3/- oxybi s- 162 C8H18O3 054305-61-2 50 4 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 'Abundance Scan 685 (11.331 min): 29518.D (-) m/z 59.05 100 . 00%

j 5000

■ I ' ' ■ ' l ' -— 45

53 60—— TT 73

83 89 103

। 114 J30.......... JU 11.00 11.20 11.40 11.60 m/z 47.82% miz-> 20 30 40 50 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 11 00 11.20 11.40 11.60 73 31 m/z 103.00. 33.79% ..... —.... TT > > Ti .... ,.......... 130.... miz-> 20 30 40 50 60 76 80 90 100 110 120 130 140 Abundance #6087; 2-Propanol. 1,1-oxybis- 59 V . / । . Tr । , Ti । 11.00 11.20 11.40 11.60 31 5000 45 m/z 73.00 27.91% 103 89 I miz-> Abundance ‘I1 20 1 : . ' I ' ' ' ' I ' ' ' ' I ' ‘ 30 40 50 1.. 72 ' I ' ' ' ' I 1 1 60 #12859: 2-Butanol, 3,3'-oxybis- 59 70 80 90 100 110 120 130 140 I ' 1 1 ' I 11.00 11.20 V TTl ■ ■ • ■ l ■ ■ ■ 1 r 11.40 A 11.60 m/ z 41.05 23.61% 5000 - 31 45 103

----- # ■ i ■ .............................. 134 , ti m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29518.D GCMS1126.M Fri Dec 21 13:13:01 2001 Page 2

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