GCMS analysis comments for sample AD29464 with phthalate detection, Jan

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC1301\29518.D Vial: 10 Acq On 13 Dec 2001 6:40 pm Operator: 209 GALOS Sample gems scan 12/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.41 3.46 ug/1 1331820 1,4 -Dichlorobenzene-d4. 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3 -oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol, -(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59 4 2-Propanol, -(2-methoxypropoxy)- 148 C7H1603 _______ 013429-07-7 50 Abundance Scan 694 (11.414 min): 29518.D (-) m/z 59.05 100.00% 59

....... .......................... 5000 45 103 73 11.20 11.40 11.60 11.80 I ' i ' 1 1 1 i ' , 2l——53—— TT— 81 89 d — 4 110 130 11.00 m/ z 44.95 45.88%

UA m/z-> 20 30 40 50 60 70 80 90 100 120 130 140 'Abundance #9238: 2-Propanol, 1-{2-methoxy-1-methylethoxy)- 59

5000

31

-------I-- ——1 45 73 103

130 m/z I 11.00 11.20 11.40 11.60 11.80 35.57%

m/z-> 20 30 40 50 60 70 80 90__ 100___11 0 120 130 140 Abundance #12859: 2-Butanol, 3,3°-oxybis- 5.9 11.00 11.20 11.40 11.60 11.80 m/z 73,00 27.29%

A 5000 31 45 103

_________1! i. ................... 134 ‘i" ' i ■ ' 1 ' i ' 1 ' ' i ' ' ■ ' i ' ' ' ' i ‘ ' i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 11.00 11.20 11.40 11.60 11.80 m/ z 41,05 24.13%

NN 5000 31 45 103

75 89 ii ■ ।' ■ ■ ■ ।' ■ ’ ■ ।1 ■ ■ ■ ।1 TI —T ........... . ' I....... . ' ' I ' ' ' ' I ' ' I I I I I I I I ' mi 20 30 40 50 60 70 80 90 100 110 120 1 3G 140 11.00 11.20 11.40 11.60 11.80

29518.D GCMS1126.M Fri Dec 21 13:13:05 2001 Page 3

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