GCMS comments for sample AD29187, Jan 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\DEC1301\29187.D Vial: 6 Acq On : 13 Dec 2001 2:44 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.598 274 278 301 rBV 383290 1045471 11.56% 2.130% 2 11.334 681 685 690 rBV 194718 401675 4.44% 0.818% 3 11.417 690 694 714 rVB 201946 526995 5.83% 1.074% 4 11.674 714 722 739 rBV2 2747581 7301282 80.71% 14.877% 5 15.273 1108 1114 1132 rBV 3842672 8465843 93.59% 17.250%

6 20.551 1683 1689 1712 rBV 4015674 9045940 100.00% 18.432% 7 24.976 2164 2171 2182 rBV2 3900813 8430455 93.20% 17.178% 8 25.114 2183 2186 2196 rVB 41933 126178 1.39% 0.257% 9 30.053 2718 2724 2731 rBV 290902 614711 6.80% 1.253% 10 31.641 2892 2897 2902 rBV 40451 92884 1.03% 0.189%

11 32.633 3000 3005 3013 rBV 78627 195595 2.16% 0.399% 12 33.009 3037 3046 3062 rBV2 2485143 6049502 66.88% 12.326% 13 33.284 3071 3076 3084 rVB 42455 111113 1.23% 0.226% 14 33.587 3103 3109 3119 rBV 117747 317331 3.51% 0.647% 15 34.515 3204 3210 3224 rBV 150136 422638 4.67% 0.861%

16 35.405 3301 3307 3319 rBV 167554 491758 5.44% 1.002% 17 35.570 3319 3325 3337 rW 98696 320361 3.54% 0.653% 18 36.259 3395 3400 3414 rBV 128579 434323 4.80% 0.885% 19 37.103 3484 3492 3520 rBV3 1493439 4683261 51.77% 9.543%

Sum of corrected areas: 49077316

29187.D GCMS1126.M Fri Dec 21 13:05:10 2001

NYC-WTC_000036518