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GCMS analysis log for sample AD30696, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.

NYC-WTC_000018123–000018141

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018128
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C: \HPCHEM\ 1 \DATA\DEC3 101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample : gems scan 12/19 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.612 276 280 294 rBV 318465 943062 14.53% 2.765% 2 11.128 658 663 671 rBV 45095 109102 1.68% 0.320% 3 11.450 694 698 714 rVB 28683 129592 2.00% 0.380% 4 11.670 717 722 753 rBV 1790757 5107476 78.70% 14.974% 5 14.305 1003 1009 1019 rBV 37810 102757 1.58% 0.301%

6 15.278 1109 1115 1135 rBV 2266967 6072123 93 .’56% 17.802% ' 7 20.566 1684 1691 1703 rBV 2343006 6490040 100.00% 19.027% 8 24.981 2166 2172 2211 rBV2 1827386 6236519 96.09% 18.284% 9 30.067 2720 2726 2737 rBV 333136 773888 11.92% 2.269% 10 33.023 3041 3048 3074 rBV2 1313776 4039170 62.24% 11.842%

11 33.602 3106 3111 3120 rBV2 26241 70652 1.09% 0.207% 12 34.520 3206 3211 3221 rBV 41424 124598 1.92% 0.365% 13 35.410 3302 3308 3318 rBV2 73800 229449 3.54% 0.673% 14 35.575 3320 3326 3335 rW 74592 223162 3.44% 0.654% 15 36.273 3396 3402 3424 rBV 107564 403635 6.22% 1.183%

16 37.118 3487 3494 3521 rBV2 612162 2823340 43.50% 8.277% 17 38.238 3608 3616 3623 rBV3 38012 154738 2.38% 0.454% 18 39.459 3741 3749 3759 rBV3 17016 76761 1.18% 0.225%

Sum of corrected areas: 34110064

30696.D GCMS1126.M Wed Jan 23 08:36:15 2002

NYC-WTC_000018128

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NYC-WTC_000018128Source: NYC Law Department, mirrored locally

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