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GC/MS analysis results for sample AD30907, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.

NYC-WTC_000018664–000018683

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

s Data File C:\HPCHEM\1\DATA\DEC3101\30907.D Vial: 43 Acq On 2 Jan 2002 5:37 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 275 279 291 rBV 209063 740906 12.95% 2.354% 2 11.133 658 663 671 rVB 25528 68260 1.19% 0.217% 3 11.675 717 722 750 rBV 1240354 4168848 72.86% 13.248% 4 14.310 1003 1009 1021 rVB 234416 567708 9.92% 1.804% 5 15.283 1109 1115 1135 rBV 1640455 5006930 87.50% 15.911%

6 17.458 1346 1352 1360 rBV 453366 1076714 18.82% 3.422% 7 18.165 1424 1429 1438 rBV2 24994 67030 1.17% 0.213% 8 20.277 1653 1659 1669 rBV 352249 780684 13.64% 2.481% 9 20.561 1684 1690 1717 rBV 2102548 5722114 100.00% 18.184% 10 21.085 1741 1747 1763 rBV3 66857 340646 5.95% 1.083%'

11 22.792 1927 1933 1941 rBV 211588 475331 8.31% 1.511% 12 24.986 2163 2172 2204 rBV2 1532413 5539741 96.81% 17.604% 13 26.896 2373 2380 2385 rBV 89929 197305 3.45% 0.627% 14 28.658 2565 2572 2578 rBV 60165 137391 2.40% 0.437% 15 30.063 2720 2725 2736 rBV2 279103 677184 11.83% 2.152%

16 30.256 2739 2746 2754 rVB 46518 117618 2.06% 0.374% 17 31.715 2899 2905 2914 rVB 36245 91443 1.60% 0.291% 18 33.028 3041 3048 3074 rBV 1061327 3563118 62.27% 11.323% 19 37.123 3487 3494 3523 rBV 496878 2129394 37.21% 6.767%

Sum of corrected areas: 31468365

30907.D GCMS1126.M Fri Jan 25 11:35:09 2002

NYC-WTC_000018669

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NYC-WTC_000018669Source: NYC Law Department, mirrored locally

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