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GCMS analysis log for sample AD30605, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.

NYC-WTC_000018194–000018213

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018199
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC3101\30605.D Vial: 30 Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal :• TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 275 279 292 rBV 342886 986083 13.82% 2.588% 2 7.755 292 295 309 rVB3 40592 167564 2.35% 0.440% 3 11.133 657 663 674 rVB 149484 376134 5.27% 0.987% 4 11.675 717 722 753 rBV 1936045 5118036 71.72% 13-431% 5 14.310 1002 1009 1018 rBV 252380 584627 8.19% 1.534%

6 15.283 1109 1115 1137 rBV 2293379 6335924 88.79% 16.628% 7 17.458 1345 1352 1362 rBV 331813 794551 11.13% 2.085% 8 20.277 1653 1659 1667 rBV 236636 517436 7.25% 1.358% 9 20.561 1683 1690 1721 rBV 2719186 7136161 100.00% 18.728% 10 21.094 1742 1748 1760 rBV 30809 146982 2.06% 0.386% 11 22.792 1927 1933 1942 rBV 143648 318773 4.47% 0.837% 12 24.986 2163 2172 2205 rBV 2148032 6860871 96.14% 18.005% 13 26.896 2374 2380 2387 rVB 61715 135807 1.90% 0.356% 14 28.658 2566 2572 2580 rVB 44499 102614 1.44% 0.269% 15 30.063 2719 2725 2739 rBV 381047 899515 12.61% 2.361% 16 30.247 2741 2745 2752 rVB2 38536 89742 1.26% 0.236% 17 31.715 2899 2905 2914 rVB 32915 76118 1.07% 0.200% 18 33.028 3041 3048 3069 rBV2 1478253 4587906 64.29% 12.040% 19 37.123 3486 3494 3522 rBV 740205 2869995 40.22% 7.532%

Sum of corrected areas: 38104839

30605.D GCMS1126.M Wed Jan 23 08:28:14 2002

NYC-WTC_000018199

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NYC-WTC_000018199Source: NYC Law Department, mirrored locally

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