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GC/MS analysis results for sample AD30935, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.

NYC-WTC_000018754–000018774

Folder label: “GCMS X 12/19/01 A 1/2/02

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Scanned page image, NYC-WTC_000018759
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NYC 9/11 Public Portal Document LSC Area Percent Report

/Data File C:\HPCHEM\1\DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 295 rBV 367133 1084265 14.88% 2.668% 2 11.128 658 663 671 rBV 29287 77778 1.07% 0.191% 3 11.670 717 722 754 rBV 1842414 5319449 72.99% 13.092% 4 14.305 1001 1009 1020 rBV 234603 569671 7.82% 1.402% 5 15.278 1110 1115 1137 rBV 2447379 6504222 89.24% 16.007%

6 17.454 1342 1352 1361 rBV 499249 1126586 15.46% 2.773% 7 18.161 1423 1429 1437 rBV 41663 97476 1.34% 0.240% 8 20.281 1654 1660 1670 rBV 359408 822746 11.29% 2.025% 9 20.557 1684 1690 1714 rBV 2687719 7288230 100.00% 17.937% 10 21.062 1739 1745 1763 rBV2 87234 447882 6.15% 1.102%

11 22.787 1927 1933 1942 rBV 220660 515651 7.08% 1.269% 12 24.982 2163 2172 2209 rBV2 2203870 7219452 99.06% 17.768% 13 26.891 2374 2380 2386 rBV 112096 240853 3.30% 0.593% 14 28.654 2563 2572 2580 rBV 76446 175665 2.41% 0.432% 15 30.067 2720 2726 2736 rBV 364904 866527 11.89% 2.133%

16 30.251 2740 2746 2752 rW 62159 143347 1.97% 0.353% 17 31.720 2898 2906 2912 rBV 46936 120565 1.65% 0.297% 18 33.023 3041 3048 3070 rBV2 1579020 4834955 66.34% 11.899% 19 34.373 3188 3195 3203 rBV 25600 73061 1.00% 0.180% 20 37.118 3486 3494 3525 rBV 798815 3104446 42.60% 7.640%

Sum of corrected areas: 40632827

30935.D GCMS1126.M Fri Jan 25 11:50:01 2002

NYC-WTC_000018759

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NYC-WTC_000018759Source: NYC Law Department, mirrored locally

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