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GC/MS analysis results for sample AD30934, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.

NYC-WTC_000018733–000018753

Folder label: “GCMS X 12/19/01 A 1/2/02

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Scanned page image, NYC-WTC_000018738
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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12 /19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 275 279 315 rBV 299320 1107572 16.14% 2.868% 2 11.134 658 663 670 rBV 31549 83126 1.21% 0.215% 3 11.675 717 722 741 rBV 1688942 4903454 71.44% 12.699% 4 14.310 1003 1009 1022 rBV2 304291 715264 10.42% 1.852% 5 15.283 1109 1115 1151 rBV 2138234 6304572 91.85% 16.327%

6 17.459 1344 1352 1362 rBV2 593716 1379610 20.10% 3.573% 7 18.166 1422 1429 1437 rBV 41071 106110 1.55% 0.275% 8 20.277 1654 1659 1668 rBV 435574 964045 14.04% 2.497% 9 20.562 1684 1690 1716 rBV 2512506 6864062 100.00% 17.776% 10 21.067 1739 1745 1763 rBV3 91794 517827 7.54% 1.341% 11 22.793 1927 1933 1945 rBV 256708 579315 8.44% 1.500% 12 24.987 2164 2172 2188 rBV2 1941889 6411412 93.41% 16.604% 13 25.143 2188 2189 2203 rVB 109964 200181 2.92% 0.518% 14 26.896 2374 2380 2386 rBV 102503 229804 3.35% 0.595% 15 28.659 2564 2572 2579 rBV 71628 158578 2.31% 0.411%

16 30.073 2720 2726 2740 rBV 317596 775978 11.30% 2.010% 17 30.256 2740 2746 2751 rW 52998 129757 1.89% 0.336% 18 31.716 2900 2905 2915 rBV 39087 102401 1.49% 0.265% 19 33.029 3040 3048 3070 rBV 1376229 4350647 63.38% 11.267% 20 37.123 3486 3494 3523 rBV2 653073 2730030 39.77% 7.070%

Sum of corrected areas: 38613745

30934.D GCMS1126.M Fri Jan 25 11:46:18 2002

NYC-WTC_000018738

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NYC-WTC_000018738Source: NYC Law Department, mirrored locally

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