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GCMS analysis summary, sample AD27288, Dec 2001

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.

NYC-WTC_000016096–000016117

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\ JANO802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.470 260 264 295 rBV 328271 1057648 15.45% 2.646% 2 10.996 644 648 656 rVB 33054 76278 1.11% 0.191% 3 11.528 701 706 731 rBV 1911552 5050481 73.76% 12.634% 4 14.172 983 994 1000 rBV 338103 662556 9.68% 1.657% 5 15.127 1092 1098 1112 rBV 2956374 6302069 92.04% 15.765%

6 17.312 1326 1336 1345 rBV2 657737 1350097 19.72% 3.377% 7 18.009 1407 1412 1419 rBV 89578 171766 2.51% 0.430% 8 20.130 1638 1643 1651 rVB 480867 969150 14.15% 2.424% 9 20.396 1665 1672 1682 rBV 3092772 6699461 97.85% 16.759% 10 20.855 1716 1722 1737 rBV 365671 752340 10.99% 1.882%

11 22.636 1910 1916 1923 rBV 298423 590112 8.62% 1.476% 12 24.803 2146 2152 2165 rBV2 3092764 6846760 100.00% 17.128% 13 24.950 2165 2168 2184 rVB2 24210 77927 1.14% 0.195% 14 26.740 2357 2363 2369 rBV 120658 247376 3.61% 0.619% 15 28.502 2549 2555 2562 rVB 87459 180998 2.64% 0.453%

16 29.889 2700 2706 2713 rBV 397553 808993 11.82% 2.024% 17 30.100 2722 2729 2736 rBV 63600 146245 2.14% 0.366% 18 31.559 2883 2888 2898 rBV 44446 106061 1.55% 0.265% 19 32.835 3019 3027 3034 rBV2 1993500 4588803 67.02% 11.479% 20 32.936 3035 3038 3051 rVB2 45807 141894 2.07% 0.355%

21 36.902 3463 3470 3488 rBV2 1131398 3148040 45.98% 7.875%

Sum of corrected areas: 39975055

27288.D GCMS1126.M Mon Feb 04 15:22:34 2002

NYC-WTC_000016101

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NYC-WTC_000016101Source: NYC Law Department, mirrored locally

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