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GCMS analysis results for sample AD29670, Jan 2002

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GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036842–000036859

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\JAN0302\29670.D Vial: 15 Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak %. of # min scan scan scan TY height area % max. total

1 7.471 260 264 276 rBV ’ 546035 1444091 12.41% 2.352% 2 7.609 276 279 297 rVB 66381 258300 2.22% 0.421% 3 10.997 642 648 657 rBV 191209 447407 3.84% 0.729% 4 11.198 667 670 675 rBV 118342 245427 2.11% 0.400% 5 11.281 675 679 693 rVB 137421 340087 2.92% 0.554%

6 11.529 699 706 723 rBV 3715822 9528707 81.87% 15.522% 7 14.164 983 993 998 rBV 241452 497134 4.27% 0.810% 8 15.128 1091 1098 1115 rBV 5285127 11346535 97.49% 18.483% 9 17.303 1328 1335 1340 rBV2 231109 455925 3.92% 0.743% 10 20.122 1633 1642 1648 rBV 132819 263340 2.26% 0.429%

11 20.397 1664 1672 1688 rBV 5384640 11638464 100.00% 18.959% 12 20.856 1718 1722 1733 rVB 57077 120079 1.03% 0.196% 13 22.637 1909 1916 1922 rBV 77528 152636 1.31% 0.249% 14 24.813 2146 2153 2165 rBV2 5041503 11169842 95.97% 18.195% 15 29.880 2700 2705 2712 rBV 503382 1016855 8.74% 1.656%

16 32.846 3020 3028 3042 rBV2 3092454 743129G 63.85% 12.105% 17 36.913 3462 3471 3491 rBV2 1847268 5032849 43.24% 8.198%

Sum of corrected areas: 61388968

29670.D GCMS1126.M Wed Jan 16 14:50:13 2002

NYC-WTC_000036847

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NYC-WTC_000036847Source: NYC Law Department, mirrored locally

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