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GCMS analysis results for sample AD29667, Jan 2002

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GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036815–000036830

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

- Data- File C:\HPCHEM\1\DATA\DEC31O1\29667 .D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.604 275 279 292 rBV 356136 1098188 10.28% 2.004% 2 11.129 658 663 674 rBV 121921 321307 3.01% 0.586% 3 11.358 684 688 693 rBV 51152 130664 1.22% 0.238% 4 11.441 693 697 705 rW 49139 142437 1.33% 0.260% 5 11.670 717 722 757 rBV 2758183 8400084 78.60% 15.328%

6 14.305 1004 1009 1018 rBV 149922 378391 3.54% 0.690% 7 15.278 1110 1115 1134 rBV 3827265 10018420 93.75% 18.281% 8 17.454 1346 1352 1361 rBV2 146051 351731 3.29% 0.642% 9 20.282 1654 1660 1666 rBV 90234 201815 1.89% 0.368% 10 20.566 1684 1691 1717 rBV 4134069 10686816 100.00% 19.501%

11 22.797 1928 1934 1942 rVB 48222 114755 1.07% 0.209% 12 24.982 2166 2172 2214 rBV2 3335206 10239424 95.81% 18.684% 13 30.068 2720 2726 2737 rBV 429436 985641 9.22% 1.799% 14 33.024 3041 3048 3074 rBV2 2431958 7062832 66,. 09% 12.888% 15 37.118 3485 3494 3528 rBV2 1280331 4670267 43.70% 8.522%

Sum of corrected areas: 54802772

29667.D GCMS1126.M Wed Jan 16 14:47:23 2002

NYC-WTC_000036820

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NYC-WTC_000036820Source: NYC Law Department, mirrored locally

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