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GCMS analysis results for sample AD30984, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.

NYC-WTC_000018248–000018261

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC3101\30984.D Vial: 38 Acq On 2 Jan 2002 12:47 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 276 279 294 rBV 427404 1170872 2.54% 1.272% 2 11.125 656 662 676 rBV 227280 572193 1.24% 0.622% 3 11.675 717 722 753 rBV 2299215 5763943 12.51% 6.261% 4 14.310 998 1009 1017 rBV 385329 945584 2.05% 1.027% 5 15.274 1109 1114 1153 rBV 2752112 7391966 16.04% 8.029%

6 17.450 1344 1351 1361 rBV2 483153 1144587 2.48% 1.243% 7 20.277 1652 1659 1668 rBV 332280 756475 1.64% 0.822% 8 20.562 1683 1690 1715 rBV 3188298 8221355 17.84% 8.930% 9 24.987 2163 2172 2213 rBV2 2544562 8142516 17.67% 8.845% 10 30.054 2718 2724 2736 rBV 965108 2200992 4.78% 2.391%

11 33.020 3040 3047 3067 rBV2 1976251 5810633 12.61% 6.312% 12 35.599 3317 3328 3373 rBV 12846700 46074203 100.00% 50.047% 13 37.123 3486 3494 3517 rBV 1085926 3866663 8.39% 4.200%

Sum of corrected areas: 92061982

30984.D GCMS1126.M Wed Jan 23 08:53:05 2002

NYC-WTC_000018253

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NYC-WTC_000018253Source: NYC Law Department, mirrored locally

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