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GCMS analysis results for sample AD30118, Jan 2002

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GCMS analysis of environmental sample AD30118 conducted January 9, 2002.

NYC-WTC_000016783–000016794

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File C:\HPCHEM\1\DATA\JAN0302\30118.D Vial: 11 Acq On 3 Jan 2002 8:20 pm Operator: 209 GALOS Sample gems scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.474 261 265 276 rBV 374519 954952 12.40% 2.379% 2 7.603 276 279 297 rVB 61980 241188 3.13% 0.601% 3 11.211 669 672 678 rBV 38538 89474 1.16% 0.223% 4 11.293 678 681 695 rVB 39230 113579 1.47% 0.283% 5 11.523 701 706 725 rBV 2316880 5986785 77.71% 14.916%

6 14.167 988 994 1000 rBV2 67840 133170 1.73% 0.332% 7 15.121 1092 1098 1117 rBV 3509989 7334609 95.20% 18.274% 8 17.306 1326 1336 1344 rBV 104162 205232 2.66% 0.511% 9 20.125 1637 1643 1648 rBV 77780 145567 1.89% 0.363% 10 20.391 1665 1672 1690 rBV 3702954 7704129 100.00% 19.195%

11 22.640 1912 1917 1925 rVB 52651 105255 1.37% 0.262% 12 24.807 2146 2153 2165 rBV2 3511676 7475614 97.03% 18.625% 13 24.954 2165 2169 2180 rVB2 26167 87109 1.13% 0.217% 14 26.826 2367 2373 2382 rBV 56334 104436 1.36% 0.260% 15 29.883 2701 2706 2713 rBV 436677 855819 11.11% 2.132%

16 32.839 3021 3028 3051 rBV2 2209878 5160504 66.98% 12.857% 17 36.906 3463 3471 3487 rBV2 1245015 3439056 44.64% 8.568%

Sum of corrected areas: 40136478

30118.D GCMS0103.M Mon Jan 07 10:36:20 2002

NYC-WTC_000016788

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NYC-WTC_000016788Source: NYC Law Department, mirrored locally

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