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GC/MS analysis results for sample AD30705, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.

NYC-WTC_000018605–000018623

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC3101\30705.D Vial: 46 Acq On : 2 Jan 2002 9:30 am Operator: 209 GALOS Sample : gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF. Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 275 280 313 rBV 263635 1031923 15.99% 3.035% 2 11.669 717 722 760 rBV 1526917 4811452 74.54% 14.1.50% 3 14.304 1004 1009 1019 rBV2 134543 333134 5.16% 0.980% 4 15.277 1110 1115 1150 rBV 2032424 5912767 91.60% 17.389% 5 17.453 1346 1352 1364 rBV 291762 684451 10.60% 2.013%

6 20.281 1654 1660 1671 rBV 233658 527618 8.17% 1.552% 7 20.565 1684 1691 1721 rBV 2371697 6455196 100.00% 18.984% 8 21.088 1742 1748 1756 rBV2 49357 217222 3.37% 0.639% 9 22.796 1928 1934 1940 rBV 147140 328226 5.08% 0.965%, 10 24.990 2163 2173 2205 rBV2 1819120 6124557 94.88% 18.012%

11 26.220 2302 2307 2318 rVB2 57103 134956 2.09% 0.397% 12 26.890 2373 2380 2387 rBV 63251 142875 2.21% 0.420% 13 28.653 2567 2572 2580 rVB 44954 101462 1.57% 0.298% 14 30.067 2720 2726 2734 rBV 310131 697226 10.80% 2.050% 15 30.250 2740 2746 2751 rBV 38575 90416 1.40% 0.266%

16 31.710 2900 2905 2912 rBV3 40933 97225 1.51% 0.286% 17 33.023 3041 3048 3070 rBV2 1266681 3948772 61.17% 11.613% 18 37.117 3487 3494 3522 rBV2 581680 2363843 36.62% 6.952%

Sum of corrected areas: 34003321

30705.D GCMS1126.M Fri Jan 25 11:26:43 2002

NYC-WTC_000018610

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