GCMS analysis comments, sample AD29137, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29137.D Vial: 33 Acq On : 11 Dec 2001 7:54 pm Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

7.74 0.76 ug/1 210813 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1, 1-trichloro- 160 C3H3C130 000918-00-3 72 2 2 - Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 10 3 1-Eicosanol 298 C20H42O 000629-96-9 9 4 Ethanol, ,2,2-trichloro­ 148 C2H3C13O 000115-20-8 9 Abundance Scan 294 (7.743 min): 29137.D () m/z 4 795 100.00% 43

5000 4 I r। : : ji T 11 rr 1k,

m/z~> 111 11 20 63 7112 m/z 124.85 40 60 80 100 120 140 160 180 200 220 240 260 280 7.40 7.60 7.80 8.00 8.81% Abundance ” #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 ■ »i • • * • । 7.40 7.60 7.80 8.00 15 m/z 96.95 5.76% 85 97 125 —at .T miz-> 20 40 60 80 100 120' 140 160 180 ‘ 200 ’ 220 240 ‘260' 280 Abundance #4368: 2-Propanone. 1,1-dichloro- 43 - 7.40 7.60 7.80 8.00 ■ 1 • ■ • ■ ।

5000 m/ Z 82.85 5.59%

15 27 63 76 93 : -m-p TUTTTITTRTI ri p ri i । 1 ri 1 [ 1 | 1 1 | 1 1 1 1 p 1 > 1 । t > 1 ■ p ri 1 ! ■ 1 miz-? Abundance 20 40 60

43 57 80 100 120 140 160 180 200 220 240 260 280 #42525:1-Eicosanol D..... LMe... 7.40 7.60 7.80 8.00 m/z 46.90 5.47% 5000 83 71 27 97

I , TT-p-m-pT "It _ ................................ 280 Mww MvA —IIBBI—nn/ TTTIr II * । . p miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.40 7.60 7.80 8.00

29137.D GCMS1126.M Wed Dec 12 15:54:31 2001 Page 2

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