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GCMS calibration table, December 2001

Machine-extracted title · confidence 95%

Calibration data sheet for GC/MS analysis dated December 28, 2001, listing deuterated standards.

NYC-WTC_000035518–000035527

Folder label: “GCMS X 11/28/01 A 12/28/01

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Scanned page image, NYC-WTC_000035522
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2801\LB.D Vial: 2 Acq On : 28 Dec 2001 8:48 am Operator: GALOS Sample : gems unknown 11/28 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.009 11 18 22 rBV 57767 100760 1.82% 0.354% 2 7.733 311 315 319 rBV 111181 194336 3.52% 0.683% 3 7.806 319 323 337 rVB 478450 971190 17.58% 3.415% 4 11.822 756 761 775 rVB 2037745 4147610 75.09% 14.584% 5 15.435 1148 1155 1170 rBV 2499770 5523400 100.00% 19.422%

6 20.708 1722 1730 1741 rBV 2526084 5229386 94.68% 18.388% 7 25.119 2204 2211 2218 rBV2 2377561 4982335 90.20% 17.519% 8 33.115 3077 3083 3098 rBV2 1837927 4105738 74.33% 14.437% 9 33.381 3107 3112 3121 rBV 68505 155511 2.82% 0.547% 10 37.196 3520 3528 3546 rVB2 1149132 3029021 54.84% 10.651%

Sum of corrected areas: 28439287

LB.D NP112701.M Mon Dec 31 10:12:08 2001

NYC-WTC_000035522

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NYC-WTC_000035522Source: NYC Law Department, mirrored locally

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