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Document / 11 pages

GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28309 analyzed on January 3, 2002.

NYC-WTC_000035411–000035421

Folder label: “GCMS X 11/26/01 A 12/22/01

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Scanned page image, NYC-WTC_000035417
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28310.D Vial: 42 Acq On : 22 Dec 2001 6:32 pm Operator: GALOS Sample : gems unknown 11/26 Inst :.GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.978 10 15 20 rVB 66106 123836 1.86% 0.359% 2 7.692 308 311 316 rBV 52024 98414 1.48% 0.285% 3 7.766 316 319 329 rVB 171798 340565 5.11% 0.986% 4 11.782 752 757 772 rVB 2553746 5149817 77.32% 14.916% 5 15.395 1144 1151 1165 rBV 3111410 6660787 100.00% 19.293%

6 20.668 1719 1726 1745 rBV 2999780 6498227 97.56% 18.822% 7 25.079 2199 2207 2218 rBV2 2833953 6191222 92.95% 17.933% 8 33.084 3073 3080 3095 rBV2 2243706 5082797 76.31% 14.722% 9 33.350 3104 3109 3118 rBV 268639 574470 8.62% 1.664% 10 37.156 3515 3524 3540 rBV2 1429588 3804666 57.12% 11.020%

Sum of corrected areas: 34524801

28310.D NP112701.M Fri Dec 28 09:10:30 2001

NYC-WTC_000035417

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NYC-WTC_000035417Source: NYC Law Department, mirrored locally

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