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GCMS analysis results for sample AD28170, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28170 conducted on January 2, 2002.

NYC-WTC_000034686–000034695

Folder label: “GCMS X 11/23/01 A 12/21/01

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Scanned page image, NYC-WTC_000034692
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28166.D Vial: 16 Acq On : 22 Dec 2001 8:30 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.968 7 14 19 rVB2 44196 89014 1.36% 0.271% 2 6.499 177 181 190 rBV 43182 94678 1.44% 0.288% 3 7.756 314 318 325 rBV 506132 975363 14.88% 2.968% 4 11.781 752 757 768 rBV 2457011 5007671 76.42% 15.237% 5 15.394 1144 1151 1168 rBV 3055748 6552931 100.00% 19.939%

6 20.667 1719 1726 1745 rBV 2927301 6235118 95.15% 18.972% 7 25.078 2200 2207 2219 rBV2 2713027 5884929 89.81% 17.906% 8 33.083 3073 3080 3094 rBV2 2092614 4636216 70.75% 14.107% 9 37.155 3516 3524 3536 rBV2 1275006 3388998 51.72% 10.312%

Sum of corrected areas: 32864918

28166.D NP112701.M Fri Dec 28 09:57:31 2001

NYC-WTC_000034692

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NYC-WTC_000034692Source: NYC Law Department, mirrored locally

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