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GCMS analysis results for sample AD28047, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD28047 conducted on January 2, 2002.

NYC-WTC_000034505–000034515

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28047.D Vial: 31 Acq On : 21 Dec 2001 10:28 pm Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min ’ scan scan scan TY height area % max. total

1 4.980 8 15 20 rVB 54318 105517 1.32% 0.261% 2 7.703 308 312 316 rBV 73081 129307 1.62% 0.319% 3 7.776 316 320 334 rVB 421434 858550 10.78% 2.121% 4 11.793 753 758 775 rVB 2976846 6077482 76.29% 15.011% 5 15.406 1145 1152 1167 rBV 3629027 7966190 100.00% 19.676%

6 20.679 1719 1727 1744 rBV 3417696 7649339 96.02% 18.893% 7 25.090 2199 2208 2218 rBV2 3228979 7240802 90.89% 17.884% 8 33.095 3073 3081 3094 rBV2 2566656 5937961 74.54% 14.666% 9 37.167 3515 3525 3538 rBV2 1637280 4522266 56.77% 11.170%

Sum of corrected areas: 40487414

28047.D NP112701.M Thu Dec 27 08:38:52 2001

NYC-WTC_000034511

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NYC-WTC_000034511Source: NYC Law Department, mirrored locally

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