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GCMS analysis results for sample AD28049, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28049 conducted on January 2, 2002.

NYC-WTC_000034548–000034558

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28049.D Vial: 34 Acq On : 22 Dec 2001 12:17 am Operator: GALOS Sample : gems unknown 11/21 Inst :.GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.977 8 15 18 rBV 41998 81135 1.02% 0.202% 2 7.700 309 312 316 rBV 48775 87464 1.10% 0.217% 3 7.774 316 320 336 rVB 356857 727811 9.17% 1.808% 4 11.799 753 759 772 rVB 2889210 6091692 76.74% 15.131% 5 15.403 1145 1152 1169 IBV 3547701 7938209 100.00% 19.718%

6 20.685 1720 1728 1743 rBV 3353243 7631059 96.13% 18.955% 7 25.087 2200 2208 2219 rBV2 3193936 7159187 90.19% 17.783% 8 33.092 3074 3081 3099 rBV2 2520923 5857734 73.79% 14.550% 9 35.623 3352 3357 3366 rBV 69471 191166 2.41% 0.475%, 10 37.164 3517 3525 3537 rBV2 1641279 4494152 56.61% 11.163%

Sum of corrected areas: 40259609

28049.D NP112701.M Thu Dec 27 08:39:29 2001

NYC-WTC_000034554

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NYC-WTC_000034554Source: NYC Law Department, mirrored locally

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