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GCMS analysis results for sample AD28167, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD28167 conducted on January 2, 2002.

NYC-WTC_000034631–000034641

Folder label: “GCMS X 11/23/01 A 12/21/01

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Scanned page image, NYC-WTC_000034637
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28104.D Vial: 11 Acq On : 22 Dec 2001 3:02 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.983 8 15 19 rVB 45345 90501 1.27% 0.246% 2 6.514 176 182 191 rW 56358 115866 1.62% 0.315% 3 7.770 315 319 332 rBV 700423 1350955 18.89% 3.672% 4 11.787 752 757 768 rBV 2556601 5488651 76.74% 14.917% 5 15.400 1144 1151 1168 rBV 3170566 7152329 100.00% 19.439%

6 20.673 1718 1726 1744 rBV 3156110 6919839 96.75% 18.807% 7 25.083 2199 2207 2218 rBV2 2906475 6473581 90.51% 17.594% 8 33.089 3073 3080 3092 rBV2 2278691 5236456 73.21% 14.232% 9 37.160 3516 3524 3538 rBV2 1446372 3965782 55.45% 10.778%

Sum of corrected areas: 36793960

28104.D NP112701.M Fri Dec 28 09:54:42 2001

NYC-WTC_000034637

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NYC-WTC_000034637Source: NYC Law Department, mirrored locally

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