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GCMS analysis results for sample AD28169, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28169 conducted on January 2, 2002.

NYC-WTC_000034706–000034717

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28169.D Vial: 19 Acq On : 22 Dec 2001 11:14 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of • # min scan scan scan TY height area % max. total

1 6.509 176 182 186 rBV 50360 97539 1.42% 0.278% 2 7.765 315 319 333 rBB 327454 630378 9.15% 1.800% 3 11.781 752 757 770 rVB 2546318 5288020 76.78% 15.097% 4 15.395 1144 1151 1166 rBV 3106665 6887671 100.00% 19.664% 5 20.667 1718 1726 1742 rBV 2971752 6690189 97.13% 19.100%

6 25.078 2199 2207 2218 rBV2 2875788 6370296 92.49% 18.187% 7 33.084 3073 3080 3095 rBV2 2267397 5165609 75.00% 14.747% 8 37.155 3516 3524 3536 rBV2 1443953 3897683 56.59% 11.128%

Sum of corrected areas: 35027385

28169.D NP112701.M Fri Dec 28 09:59:30 2001

NYC-WTC_000034712

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NYC-WTC_000034712Source: NYC Law Department, mirrored locally

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